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Leveraging infrared spectroscopy for cocoa content prediction: A dual approach with Kohonen neural network and multivariate modeling

2025, Lima, Clara Mariana Gonçalves, Silveira, Paula Giarolla, Santana, Renata Ferreira, da Piedade Edmundo Sitoe, Eugénio, Bonomo, Renata Cristina Ferreira, Coutinho, Henrique Douglas Melo, Wawrzyniak, Jolanta, de Carvalho dos Anjos, Virgílio, Bell, Maria José Valenzuela, Contado, José Luís, Zengin, Gökhan, da Rocha, Roney Alves

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Rapid Detection of Tea Adulteration Using FT-NIR Spectroscopy Combined with t-SNE Analysis

2025, Lima, Clara Mariana Gonçalves, Silveira, Paula Giarolla, Santana, Renata Ferreira, Khalid, Waseem, Mourão, Matheus da Silva, Bonomo, Renata Cristina Ferreira, Coutinho, Henrique Douglas Melo, Dos Anjos, Virgílio de Carvalho, Bell, Maria José Valenzuela, Batista, Luís Roberto, Contado, José Luís, Wawrzyniak, Jolanta, Verruck, Silvani, Da Rocha, Roney Alves

Tea is one of the most popular non-alcoholic beverages internationally, and it is not uncommon to find commercial tea preparations mixed with leaves and parts of other plants to increase profit and production volume, which constitutes fraud. The aim of this study was to perform Fourier transform-near-infrared spectroscopic characterization of leaves and pieces (petioles and stems) of three types of medicinal plants (Chamomile, Ginseng, and Quebra-pedras) used in the preparation of teas. Cluster analysis methods were used to evaluate the ability of Fourier transform-near-infrared to identify plant types, with t-SNE presenting the best discriminatory power. The deconvolution of the spectra showed that 15 vibration bands allow a good characterization of the samples, all with R² greater than 0.99.

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Empirical Modeling of the Drying Kinetics of Red Beetroot (Beta vulgaris L.; Chenopodiaceae) with Peel, and Flour Stability in Laminated and Plastic Flexible Packaging

2024, Sousa, Elisabete Piancó de, Oliveira, Emanuel Neto Alves de, Lima, Thamirys Lorranne Santos, Almeida, Rafael Fernandes, Barros, Jefferson Henrique Tiago, Lima, Clara Mariana Gonçalves, Giuffrè, Angelo Maria, Wawrzyniak, Jolanta, Wybraniec, Sławomir, Coutinho, Henrique Douglas Melo, Feitosa, Bruno Fonsêca

Despite the high global production of beetroot (Beta vulgaris L.), its peel is often discarded. Transforming beetroot into flour can reduce waste, improve food security, and decrease environmental pollution. However, large-scale feasibility depends on understanding drying kinetics and optimal storage conditions. This study aimed to investigate the effects of different temperatures in the convective drying of whole beetroot and evaluate the influence of laminated flexible and plastic packaging on flour stability over two months. Drying kinetics were analyzed using five models, with the Page and Logarithm models showing the best fit (R2 > 0.99). Def values (1.27 × 10−9 to 2.04 × 10−9 m2 s−1) increased with rising temperatures while drying time was reduced (from 820 to 400 min), indicating efficient diffusion. The activation energy was 29.34 KJ mol−1, comparable to other plant matrices. Drying reduced moisture and increased ash concentration in the flour. The flour showed a good water adsorption capacity and low cohesiveness, making it marketable. Laminated packaging was more effective in controlling physicochemical parameters, reducing hygroscopicity, and maintaining quality over 60 days. In summary, the Page model can predict beetroot drying kinetics effectively, and laminated packaging can control flour stability.