Fast analysis of terpenes using GC-TOFMS with a 50 µm ID column
| cris.virtual.author-orcid | 0000-0002-6568-8155 | |
| cris.virtualsource.author-orcid | 1ddb8111-48d2-4a19-a7fb-97562fc1691c | |
| dc.abstract.en | A method of terpenes analysis using GC-TOFMS system with a nanobore SLB-5 ms, 5 m, 50 µm ID column is described. Terpene test mixture of 46 compounds was used in analyses. In comparison to a standard column of the same phase (SLB-5 ms, 30 m, 250 µm ID) used for essential oils analysis the total analysis time of 46 compounds in a test mixture was reduced from 25.8 min to 3.8 min. Coelutions were observed in analysis on both columns – 5 and 4 for the nanobore and standard column respectively. For some coeluting compounds spectra obtained after deconvolution provided a reliable identification and possibility of their quantitation. The method uses hydrogen as a carrier gas for GC/MS, which in the shortage of helium is an attractive alternative, especially for fast GC.. The method can be used for high throughput analyses of essential oils. | |
| dc.affiliation | Wydział Nauk o Żywności i Żywieniu | |
| dc.affiliation.institute | Katedra Technologii Żywności Pochodzenia Roślinnego | |
| dc.contributor.author | Jeleń, Henryk | |
| dc.date.accessioned | 2025-10-23T09:43:48Z | |
| dc.date.available | 2025-10-23T09:43:48Z | |
| dc.date.issued | 2025 | |
| dc.description.bibliography | il., bibliogr. | |
| dc.description.finance | publication_nocost | |
| dc.description.financecost | 0,00 | |
| dc.description.if | 4,0 | |
| dc.description.points | 100 | |
| dc.description.volume | 1762 | |
| dc.identifier.doi | 10.1016/j.chroma.2025.466378 | |
| dc.identifier.eissn | 1873-3778 | |
| dc.identifier.issn | 0021-9673 | |
| dc.identifier.uri | https://sciencerep.up.poznan.pl/handle/item/5411 | |
| dc.language | en | |
| dc.relation.ispartof | Journal of Chromatography A | |
| dc.relation.pages | art. 466378 | |
| dc.rights | ClosedAccess | |
| dc.sciencecloud | nosend | |
| dc.subject.en | terpenes | |
| dc.subject.en | essential oils | |
| dc.subject.en | nanobore GC columns | |
| dc.subject.en | GC-TOFMS | |
| dc.subject.en | retention parameters | |
| dc.title | Fast analysis of terpenes using GC-TOFMS with a 50 µm ID column | |
| dc.type | JournalArticle | |
| dspace.entity.type | Publication | |
| oaire.citation.volume | 1762 |